7.3 Neutron diffraction  (Page 2/7)

Neutron detectors

Although neutrons are great particles for determining complete structures of materials they have some disadvantages. These particles experiment a reasonably weak scattering when looking especially to soft materials. This is a huge concern because there can be problems associated with the scattering of the particles which can lead to a misunderstanding in the analysis of the structure of the material.

Neutrons are particles that have the ability to penetrate through the surface of the material being examined. This is primarily due to the nuclear interaction produced from the particles and the nucleus from the material. This interaction is much greater that the one performed from the electrons, which it is only an electrostatic interaction. Also, it cannot be omitted the interaction that occurs between the electrons and the magnetic moment of the neutrons. All of these interactions discussed are of great advantage for the determination of the structure since neutrons interacts with every single nucleus in the material. The problem comes when the material is being analyzed because neutrons being uncharged materials make them difficult to detect them. For this reason, neutrons need to be reacted in order to generate charged particles, ions. Some of the reactions uusually used for the detection of neutrons are:

The first two reactions apply when the detection is performed in a gas environment whereas the third one is carried out in a solid. In each of these reaction there is a large cross section, which makes them ideal for neutron capture. The neutron detection hugely depends on the velocity of the particles. As velocity increases, shorter wavelengths are produced and the less efficient the detection becomes. The particles that are executed to the material need to be as close as possible in order to have an accurate signal from the detector. These signal needs to be quickly transduced and the detector should be ready to take the next measurement.

In gas detectors the cylinder is filled up with either ³ He or BF _3. The electrons produced by the secondary ionization interact with the positively charged anode wire. One disadvantage of this detector is that it cannot be attained a desired thickness since it is very difficult to have a fixed thickness with a gas. In contrast, in scintillator detectors since detection is developed in a solid, any thickness can be obtained. The thinner the thickness of the solid the more efficient the results obtained become. Usually the absorber is ⁶ Li and the substrate, which detects the products, is phosphor, which exhibits luminescence. This emission of light produced from the phosphor results from the excitation of this when the ions pass thorough the scintillator. Then the signal produced is collected and transduced to an electrical signal in order to tell that a neutron has been detected.

Neutron scattering

One of the greatest features of neutron scattering is that neutrons are scattered by every single atomic nucleus in the material whereas in X-ray studies, these are scattered by the electron density. In addition, neutron can be scattered by the magnetic moment of the atoms. The intensity of the scattered neutrons will be due to the wavelength at which it is executed from the source. [link] shows how a neutron is scattered by the target when the incident beam hits it.